Information card for entry 7046840

Structure parameters

• Formula: C29 H23 B F15 N Si
• Calculated formula: C29 H23 B F15 N Si
• Title of publication: Formation of borata-alkene/iminium zwitterions by ynamine hydroboration.
• Authors of publication: Wang, Long; Jian, Zhongbao; Daniliuc, Constantin G.; Kehr, Gerald; Erker, Gerhard
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 32
• Pages of publication: 10853 - 10856
• a: 12.6697 ± 0.0004 Å
• b: 17.9299 ± 0.0006 Å
• c: 13.6897 ± 0.0004 Å
• α: 90°
• β: 100.925 ± 0.001°
• γ: 90°
• Cell volume: 3053.48 ± 0.17 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0347
• Residual factor for significantly intense reflections: 0.0301
• Weighted residual factors for significantly intense reflections: 0.0722
• Weighted residual factors for all reflections included in the refinement: 0.0746
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No