Information card for entry 7046842

Structure parameters

• Formula: C46 H36 B F20 N Si Zr
• Calculated formula: C46 H36 B F20 N Si Zr
• Title of publication: Formation of borata-alkene/iminium zwitterions by ynamine hydroboration.
• Authors of publication: Wang, Long; Jian, Zhongbao; Daniliuc, Constantin G.; Kehr, Gerald; Erker, Gerhard
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 32
• Pages of publication: 10853 - 10856
• a: 11.1163 ± 0.0006 Å
• b: 13.9216 ± 0.0008 Å
• c: 14.4781 ± 0.0008 Å
• α: 88.616 ± 0.003°
• β: 88.273 ± 0.003°
• γ: 84.773 ± 0.002°
• Cell volume: 2229.7 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0555
• Residual factor for significantly intense reflections: 0.0437
• Weighted residual factors for significantly intense reflections: 0.0931
• Weighted residual factors for all reflections included in the refinement: 0.0991
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No