Information card for entry 7046844

Structure parameters

• Formula: C28 H30 B F10 N Si
• Calculated formula: C28 H30 B F10 N Si
• Title of publication: Formation of borata-alkene/iminium zwitterions by ynamine hydroboration.
• Authors of publication: Wang, Long; Jian, Zhongbao; Daniliuc, Constantin G.; Kehr, Gerald; Erker, Gerhard
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 32
• Pages of publication: 10853 - 10856
• a: 10.019 ± 0.0002 Å
• b: 19.0596 ± 0.0003 Å
• c: 15.5129 ± 0.0003 Å
• α: 90°
• β: 94.422 ± 0.001°
• γ: 90°
• Cell volume: 2953.5 ± 0.09 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0703
• Residual factor for significantly intense reflections: 0.0542
• Weighted residual factors for significantly intense reflections: 0.1216
• Weighted residual factors for all reflections included in the refinement: 0.1326
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No