Information card for entry 7046848

Structure parameters

• Formula: C56 H60 Br4 Cl16 F2 Ir N8 Rh
• Calculated formula: C56 H60 Br4 Cl16 F2 Ir N8 Rh
• Title of publication: Preparation of polynuclear NHC complexes by post-synthetic modification of half-sandwich rhodium and iridium complexes bearing C-azolato ligands.
• Authors of publication: Aznarez, Francisco; Gao, Wen-Xi; Lin, Yue-Jian; Hahn, F. Ekkehardt; Jin, Guo-Xin
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 28
• Pages of publication: 9442 - 9452
• a: 11.1069 ± 0.0014 Å
• b: 11.9474 ± 0.0015 Å
• c: 15.827 ± 0.002 Å
• α: 91.503 ± 0.002°
• β: 100.293 ± 0.002°
• γ: 100.247 ± 0.002°
• Cell volume: 2029.8 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0836
• Residual factor for significantly intense reflections: 0.0571
• Weighted residual factors for significantly intense reflections: 0.171
• Weighted residual factors for all reflections included in the refinement: 0.2118
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No