Information card for entry 7046853

Structure parameters

• Formula: C14.5 H22 Fe I2 N P
• Calculated formula: C14.5 H22 Fe I2 N P
• Title of publication: Redox behaviour of ([fc(NPⁱPr₂)₂]Fe)₂, formation of an iron-iron bond and cleavage of azobenzene.
• Authors of publication: Pick, Fraser S.; Leznoff, Daniel B.; Fryzuk, Michael D.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 32
• Pages of publication: 10925 - 10931
• a: 14.8284 ± 0.0013 Å
• b: 17 ± 0.0015 Å
• c: 14.5439 ± 0.0013 Å
• α: 90°
• β: 90.654 ± 0.002°
• γ: 90°
• Cell volume: 3666 ± 0.6 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296.15 K
• Number of distinct elements: 6
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0252
• Residual factor for significantly intense reflections: 0.0243
• Weighted residual factors for significantly intense reflections: 0.0572
• Weighted residual factors for all reflections included in the refinement: 0.0575
• Goodness-of-fit parameter for all reflections included in the refinement: 1.136
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No