Information card for entry 7046943

Structure parameters

• Formula: C40 H72 Cl N4 P3 W
• Calculated formula: C40 H72 Cl N4 P3 W
• Title of publication: The new diphosphanylphosphido complexes of tungsten(vi) and molybdenum(vi). Their synthesis, structures and properties.
• Authors of publication: Wiśniewska, A; Grubba, R.; Ponikiewski, Ł; Zauliczny, M.; Pikies, J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 30
• Pages of publication: 10213 - 10222
• a: 11.0041 ± 0.0004 Å
• b: 20.8898 ± 0.0007 Å
• c: 22.1047 ± 0.0007 Å
• α: 106.063 ± 0.003°
• β: 102.935 ± 0.003°
• γ: 101.944 ± 0.003°
• Cell volume: 4558.6 ± 0.3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.095
• Residual factor for significantly intense reflections: 0.0618
• Weighted residual factors for significantly intense reflections: 0.1476
• Weighted residual factors for all reflections included in the refinement: 0.1641
• Goodness-of-fit parameter for all reflections included in the refinement: 0.95
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No