Information card for entry 7047041

Structure parameters

• Formula: C70.23 H98.26 Co F6 N6 Sb
• Calculated formula: C70.224 H98.256 Co F6 N6 Sb
• Title of publication: Structural snapshots of the rearrangement of the bis(di-tert-butyl-aminophenyl)amine pincer ligand in the presence of transition metal ions.
• Authors of publication: Leconte, N.; Baptiste, B.; Philouze, C.; Thomas, F.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 33
• Pages of publication: 11303 - 11307
• a: 19.171 ± 0.004 Å
• b: 18.08 ± 0.004 Å
• c: 40.633 ± 0.008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 14084 ± 5 ų
• Cell temperature: 200 K
• Ambient diffraction temperature: 200 K
• Number of distinct elements: 6
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.1053
• Residual factor for significantly intense reflections: 0.0553
• Weighted residual factors for significantly intense reflections: 0.139
• Weighted residual factors for all reflections included in the refinement: 0.1597
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No