Information card for entry 7047044

Structure parameters

• Formula: C114 H174 F12 N12 O2 Sb2
• Calculated formula: C114 H174 F12 N12 O2 Sb2
• Title of publication: Structural snapshots of the rearrangement of the bis(di-tert-butyl-aminophenyl)amine pincer ligand in the presence of transition metal ions.
• Authors of publication: Leconte, N.; Baptiste, B.; Philouze, C.; Thomas, F.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 33
• Pages of publication: 11303 - 11307
• a: 13.287 ± 0.002 Å
• b: 13.328 ± 0.002 Å
• c: 17.363 ± 0.007 Å
• α: 93.48 ± 0.03°
• β: 98.319 ± 0.017°
• γ: 93.55 ± 0.02°
• Cell volume: 3029 ± 1.4 ų
• Cell temperature: 200 K
• Ambient diffraction temperature: 200 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0997
• Residual factor for significantly intense reflections: 0.0542
• Weighted residual factors for significantly intense reflections: 0.1065
• Weighted residual factors for all reflections included in the refinement: 0.1295
• Goodness-of-fit parameter for all reflections included in the refinement: 1.077
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No