Information card for entry 7047062

Structure parameters

• Common name: work
• Formula: C72 H72 B F24 N2 O P Pd
• Calculated formula: C72 H72 B F24 N2 O P Pd
• Title of publication: Phenylacetylene polymerisation mediated by cationic cyclometallated palladium(ii) complexes bearing benzylidene 2,6-diisopropylphenylamine and its derivatives as ligands.
• Authors of publication: Joseph, M. Cassiem; Swarts, Andrew J.; Mapolie, Selwyn F.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 35
• Pages of publication: 12209 - 12217
• a: 10.0762 ± 0.001 Å
• b: 18.3919 ± 0.0019 Å
• c: 19.844 ± 0.002 Å
• α: 101.149 ± 0.001°
• β: 92.522 ± 0.001°
• γ: 92.592 ± 0.001°
• Cell volume: 3599.2 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Ambient diffracton pressure: 101.3 kPa
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0446
• Residual factor for significantly intense reflections: 0.0383
• Weighted residual factors for significantly intense reflections: 0.0902
• Weighted residual factors for all reflections included in the refinement: 0.0942
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No