Crystallography Open Database

Information card for entry 7047068

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Structure parameters

Formula	C23 H26 B N4 Rh
Calculated formula	C23 H26 B N4 Rh
Title of publication	Preparation and Reactivity of Rhodium and Iridium Complexes Containing a Methylborohydride Based Unit Supported by Two 7-Azaindolyl Heterocycles
Authors of publication	Da Costa, Rosenildo Correa; Rawe, Benjamin W.; Tsoureas, Nikolaos; Haddow, Mairi F.; Sparkes, Hazel Anne; Tizzard, Graham J.; Coles, Simon; Owen, Gareth Richard
Journal of publication	Dalton Transactions
Year of publication	2018
a	14.9965 ± 0.0003 Å
b	16.0602 ± 0.0003 Å
c	16.3753 ± 0.0005 Å
α	111.475 ± 0.001°
β	107.628 ± 0.001°
γ	106.489 ± 0.001°
Cell volume	3132.32 ± 0.14 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0362
Residual factor for significantly intense reflections	0.0286
Weighted residual factors for significantly intense reflections	0.0701
Weighted residual factors for all reflections included in the refinement	0.0743
Goodness-of-fit parameter for all reflections included in the refinement	1.064
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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