Crystallography Open Database

Information card for entry 7047223

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Coordinates	7047223.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C43.5 H60 N4 P4
Calculated formula	C43.5 H59.9227 N4 P4
Title of publication	The chameleonic reactivity of dilithio bis(alkylamido)cyclodiphosph(iii)azanes with chlorophosphines.
Authors of publication	Otang, Mathew E.; Josephson, David; Duppong, Todd; Stahl, Lothar
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2018
Journal volume	47
Journal issue	33
Pages of publication	11625 - 11635
a	9.6038 ± 0.0003 Å
b	13.3765 ± 0.0003 Å
c	16.9285 ± 0.0004 Å
α	97.9385 ± 0.0014°
β	92.729 ± 0.0015°
γ	102.033 ± 0.0015°
Cell volume	2099.99 ± 0.1 Å³
Cell temperature	100.04 K
Ambient diffraction temperature	100.04 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0671
Residual factor for significantly intense reflections	0.0483
Weighted residual factors for significantly intense reflections	0.1067
Weighted residual factors for all reflections included in the refinement	0.1202
Goodness-of-fit parameter for all reflections included in the refinement	1.053
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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