Crystallography Open Database

Information card for entry 7047244

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Structure parameters

Formula	C16 H32 B2 Cl2 P2
Calculated formula	C16 H32 B2 Cl2 P2
Title of publication	Synthesis and coordination chemistry of new asymmetric donor/acceptor pincer ligands, 1,3-C<sub>6</sub>H<sub>4</sub>(CH<sub>2</sub>P<sup>t</sup>Bu(R<sub>f</sub>))<sub>2</sub> (R<sub>f</sub> = CF<sub>3</sub>, C<sub>2</sub>F<sub>5</sub>).
Authors of publication	Debnath, Suman; Venegas, Gabriel; Arulsamy, Navamoney; Roddick, Dean M.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2018
Journal volume	47
Journal issue	35
Pages of publication	12420 - 12430
a	7.1272 ± 0.0001 Å
b	13.1027 ± 0.0002 Å
c	13.4944 ± 0.0002 Å
α	118.878 ± 0.001°
β	98.466 ± 0.0001°
γ	90.718 ± 0.001°
Cell volume	1086.35 ± 0.03 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0814
Residual factor for significantly intense reflections	0.0639
Weighted residual factors for significantly intense reflections	0.1734
Weighted residual factors for all reflections included in the refinement	0.1886
Goodness-of-fit parameter for all reflections included in the refinement	1.034
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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