Information card for entry 7047246

Structure parameters

• Formula: C102 H102 B2 Cl4 N2 O6 Os2 P4
• Calculated formula: C102 H102 B2 Cl4 N2 O6 Os2 P4
• Title of publication: Preparation and reactivity of half-sandwich organic azide complexes of osmium.
• Authors of publication: Albertin, Gabriele; Antoniutti, Stefano; Castro, Jesús; Ganz, Verena; Sibilla, Francesca
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 33
• Pages of publication: 11658 - 11668
• a: 12.7763 ± 0.0019 Å
• b: 13.497 ± 0.002 Å
• c: 14.717 ± 0.002 Å
• α: 63.354 ± 0.004°
• β: 86.818 ± 0.005°
• γ: 83.617 ± 0.005°
• Cell volume: 2254.2 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0364
• Residual factor for significantly intense reflections: 0.0326
• Weighted residual factors for significantly intense reflections: 0.0849
• Weighted residual factors for all reflections included in the refinement: 0.0867
• Goodness-of-fit parameter for all reflections included in the refinement: 1.094
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No