Information card for entry 7047275

Structure parameters

• Formula: C22 H21 N2 O2 P
• Calculated formula: C22 H21 N2 O2 P
• Title of publication: Lewis and Brønsted basicity of phosphine-diazomethane derivatives.
• Authors of publication: Schneider, Carolin; LaFortune, James H. W.; Melen, Rebecca L.; Stephan, Douglas W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 36
• Pages of publication: 12742 - 12749
• a: 10.661 ± 0.004 Å
• b: 13.155 ± 0.005 Å
• c: 14.357 ± 0.006 Å
• α: 77.71 ± 0.02°
• β: 89.3 ± 0.03°
• γ: 87.78 ± 0.02°
• Cell volume: 1965.9 ± 1.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1463
• Residual factor for significantly intense reflections: 0.0619
• Weighted residual factors for significantly intense reflections: 0.1455
• Weighted residual factors for all reflections included in the refinement: 0.2079
• Goodness-of-fit parameter for all reflections included in the refinement: 0.973
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No