Crystallography Open Database

Information card for entry 7047350

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Coordinates	7047350.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H98 Si10
Calculated formula	C48 H98 Si10
Title of publication	The selective formation of a 1,2-disilabenzene from the reaction of a disilyne with phenylacetylene.
Authors of publication	Sugahara, Tomohiro; Guo, Jing-Dong; Hashizume, Daisuke; Sasamori, Takahiro; Nagase, Shigeru; Tokitoh, Norihiro
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2018
Journal volume	47
Journal issue	38
Pages of publication	13318 - 13322
a	19.8244 ± 0.0004 Å
b	12.3683 ± 0.0002 Å
c	27.2326 ± 0.0005 Å
α	90°
β	104.974 ± 0.002°
γ	90°
Cell volume	6450.5 ± 0.2 Å³
Cell temperature	103 ± 2 K
Ambient diffraction temperature	103 ± 2 K
Number of distinct elements	3
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0628
Residual factor for significantly intense reflections	0.0529
Weighted residual factors for significantly intense reflections	0.1203
Weighted residual factors for all reflections included in the refinement	0.124
Goodness-of-fit parameter for all reflections included in the refinement	1.239
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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