Information card for entry 7047413

Structure parameters

• Formula: C40 H100 O52 Rh4 W8
• Calculated formula: C40 H60 O51.9996 Rh4 W8
• Title of publication: A comprehensive approach providing a new synthetic route for bimetallic electrocatalysts via isoPOMs [M/Rh(Cp*)₄W₈O₃₂] (M = Rh (1) and Ir (2)).
• Authors of publication: Singh, Vikram; Ma, Pengtao; Drew, Michael G. B.; Wang, Jingping; Niu, Jingyang
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 39
• Pages of publication: 13870 - 13879
• a: 12.461 ± 0.002 Å
• b: 15.509 ± 0.003 Å
• c: 22.269 ± 0.004 Å
• α: 90°
• β: 99.352 ± 0.003°
• γ: 90°
• Cell volume: 4246.5 ± 1.3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0599
• Residual factor for significantly intense reflections: 0.0403
• Weighted residual factors for significantly intense reflections: 0.1017
• Weighted residual factors for all reflections included in the refinement: 0.1086
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No