Information card for entry 7047422

Structure parameters

• Formula: C23 H41 B10 Ir2 O
• Calculated formula: C23 H41 B10 Ir2 O
• Title of publication: Regioselective B-H/C-H activation and metal-metal bond formation induced by half-sandwich metals complexes at hydroxy-substituted o-carboranes.
• Authors of publication: Guo, Shu-Ting; Cui, Peng-Fei; Gao, Yang; Jin, Guo-Xin
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 38
• Pages of publication: 13641 - 13646
• a: 11.509 ± 0.004 Å
• b: 13.941 ± 0.004 Å
• c: 18.125 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2908.1 ± 1.6 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.058
• Residual factor for significantly intense reflections: 0.0448
• Weighted residual factors for significantly intense reflections: 0.1325
• Weighted residual factors for all reflections included in the refinement: 0.1442
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No