Information card for entry 7047486

Structure parameters

• Formula: C72 H60 P6 Pd4 S3
• Calculated formula: C72 H60 P6 Pd4 S3
• Title of publication: The coordination chemistry of phosphinidene sulfides. Synthesis and catalytic properties of Pd₄ and Pt₄ clusters.
• Authors of publication: Chai, Jinkui; Tian, Rongqiang; Wu, Di; Wei, Donghui; Xu, Qun; Duan, Zheng; Mathey, François
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 38
• Pages of publication: 13342 - 13344
• a: 32.9703 ± 0.0004 Å
• b: 15.48579 ± 0.00016 Å
• c: 29.9766 ± 0.0004 Å
• α: 90°
• β: 93.7902 ± 0.0011°
• γ: 90°
• Cell volume: 15271.7 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0485
• Residual factor for significantly intense reflections: 0.0361
• Weighted residual factors for significantly intense reflections: 0.0887
• Weighted residual factors for all reflections included in the refinement: 0.0937
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No