Information card for entry 7047489

Structure parameters

• Formula: C66 H54 P6 Pd4 S6
• Calculated formula: C66 H54 P6 Pd4 S6
• Title of publication: The coordination chemistry of phosphinidene sulfides. Synthesis and catalytic properties of Pd₄ and Pt₄ clusters.
• Authors of publication: Chai, Jinkui; Tian, Rongqiang; Wu, Di; Wei, Donghui; Xu, Qun; Duan, Zheng; Mathey, François
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 38
• Pages of publication: 13342 - 13344
• a: 15.607 ± 0.0003 Å
• b: 27.8868 ± 0.0003 Å
• c: 17.6155 ± 0.0003 Å
• α: 90°
• β: 112.931 ± 0.002°
• γ: 90°
• Cell volume: 7060.9 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0494
• Residual factor for significantly intense reflections: 0.0371
• Weighted residual factors for significantly intense reflections: 0.0854
• Weighted residual factors for all reflections included in the refinement: 0.0906
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No