Information card for entry 7047705

Structure parameters

• Formula: C72 H68 Ag3 B2 F4 N3 O0 P6
• Calculated formula: C72 H68 Ag3 B2 F4 N3 P6
• Title of publication: Synthesis, structure, and condensed-phase reactivity of [Ag₃(μ₃-H)(μ₃-BH₄)L^Ph₃](BF₄) (L^Ph = bis(diphenylphosphino)amine) with CS₂.
• Authors of publication: Ma, Howard Z.; White, Jonathan M.; Mulder, Roger J.; Reid, Gavin E.; Canty, Allan J.; O'Hair, Richard A J
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 41
• Pages of publication: 14713 - 14725
• a: 18.3179 ± 0.0004 Å
• b: 22.8489 ± 0.0004 Å
• c: 21.3193 ± 0.0006 Å
• α: 90°
• β: 114.712 ± 0.003°
• γ: 90°
• Cell volume: 8105.9 ± 0.4 ų
• Cell temperature: 130 ± 0.1 K
• Ambient diffraction temperature: 130 ± 0.1 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0767
• Residual factor for significantly intense reflections: 0.0538
• Weighted residual factors for significantly intense reflections: 0.1379
• Weighted residual factors for all reflections included in the refinement: 0.1549
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No