Information card for entry 7047730

Structure parameters

• Formula: C17 H24 Cl Ge N O
• Calculated formula: C17 H24 Cl Ge N O
• Title of publication: Cyclometallation of a germylene ligand by concerted metalation-deprotonation of a methyl group.
• Authors of publication: Bakthavachalam, K.; Dutta, Sayan; C, Arivazhagan; Raghavendra, Beesam; Haridas, Anagha; Sen, Sakya S.; Koley, Debasis; Ghosh, Sundargopal
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 44
• Pages of publication: 15835 - 15844
• a: 12.2217 ± 0.0005 Å
• b: 12.2217 ± 0.0005 Å
• c: 10.6077 ± 0.0007 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 1372.19 ± 0.12 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 145
• Hermann-Mauguin space group symbol: P 32
• Hall space group symbol: P 32
• Residual factor for all reflections: 0.0687
• Residual factor for significantly intense reflections: 0.0497
• Weighted residual factors for significantly intense reflections: 0.1088
• Weighted residual factors for all reflections included in the refinement: 0.1235
• Goodness-of-fit parameter for all reflections included in the refinement: 1.004
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No