Information card for entry 7047957

Structure parameters

• Formula: C20 H30 P4 Ru2
• Calculated formula: C20 H30 P4 Ru2
• Title of publication: Ruthenium mediated halogenation of white phosphorus: synthesis and reactivity of the unprecedented P₄Cl₂ moiety.
• Authors of publication: Bispinghoff, Mark; Benkő, Zoltán; Grützmacher, Hansjörg; Calvo, Fuencisla Delgado; Caporali, Maria; Peruzzini, Maurizio
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 11
• Pages of publication: 3593 - 3600
• a: 22.85 ± 0.0005 Å
• b: 22.85 ± 0.0005 Å
• c: 8.9379 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4666.7 ± 0.2 ų
• Cell temperature: 105 ± 1 K
• Ambient diffraction temperature: 105 ± 1 K
• Number of distinct elements: 4
• Space group number: 106
• Hermann-Mauguin space group symbol: P 42 b c
• Hall space group symbol: P 4c -2ab
• Residual factor for all reflections: 0.0474
• Residual factor for significantly intense reflections: 0.0354
• Weighted residual factors for significantly intense reflections: 0.0599
• Weighted residual factors for all reflections included in the refinement: 0.064
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No