Information card for entry 7048075

Structure parameters

• Formula: C60 H100 Ho K2 O15
• Calculated formula: C60 H100 Ho K2 O15
• Title of publication: Isolation of reactive Ln(ii) complexes with C₅H₄Me ligands (Cp^Me) using inverse sandwich countercations: synthesis and structure of [(18-crown-6)K(μ-Cp^Me)K(18-crown-6)][Cp^Me₃Ln^II] (Ln = Tb, Ho).
• Authors of publication: Huh, Daniel N.; Ziller, Joseph W.; Evans, William J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 48
• Pages of publication: 17285 - 17290
• a: 9.6024 ± 0.0009 Å
• b: 26.131 ± 0.002 Å
• c: 25.176 ± 0.002 Å
• α: 90°
• β: 90.7143 ± 0.0012°
• γ: 90°
• Cell volume: 6316.7 ± 0.9 ų
• Cell temperature: 88 ± 2 K
• Ambient diffraction temperature: 88 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0617
• Residual factor for significantly intense reflections: 0.0398
• Weighted residual factors for significantly intense reflections: 0.0904
• Weighted residual factors for all reflections included in the refinement: 0.0995
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No