Information card for entry 7048086

Structure parameters

• Formula: C124 H146 O20 Tb2
• Calculated formula: C124 H146 O20 Tb2
• Title of publication: Lanthanoid complexes supported by retro-Claisen condensation products of β-triketonates.
• Authors of publication: Abad Galán, Laura; Sobolev, Alexandre N.; Zysman-Colman, Eli; Ogden, Mark I.; Massi, Massimiliano
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 48
• Pages of publication: 17469 - 17478
• a: 15.0467 ± 0.0001 Å
• b: 20.8306 ± 0.0001 Å
• c: 19.1237 ± 0.0002 Å
• α: 90°
• β: 110.933 ± 0.001°
• γ: 90°
• Cell volume: 5598.37 ± 0.08 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0274
• Residual factor for significantly intense reflections: 0.0241
• Weighted residual factors for significantly intense reflections: 0.0607
• Weighted residual factors for all reflections included in the refinement: 0.0628
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No