Information card for entry 7048146
| Formula |
C69 H93 N3 O P4 |
| Calculated formula |
C69 H93 N3 O P4 |
| Title of publication |
Chiral [16]-ane P<sub>4</sub>N<sub>2</sub> macrocycles: stereoselective synthesis and unexpected intermolecular exchange of endocyclic fragments. |
| Authors of publication |
Musina, E. I.; Naumov, R. N.; Kanunnikov, K. B.; Dobrynin, A. B.; Gómez-Ruiz, S; Lönnecke, P; Hey-Hawkins, E; Karasik, A. A.; Sinyashin, O. G. |
| Journal of publication |
Dalton transactions (Cambridge, England : 2003) |
| Year of publication |
2018 |
| Journal volume |
47 |
| Journal issue |
47 |
| Pages of publication |
16977 - 16984 |
| a |
11.6268 ± 0.0004 Å |
| b |
12.1381 ± 0.0005 Å |
| c |
13.2236 ± 0.0004 Å |
| α |
88.667 ± 0.003° |
| β |
70.775 ± 0.003° |
| γ |
64.619 ± 0.004° |
| Cell volume |
1576.78 ± 0.12 Å3 |
| Cell temperature |
130 ± 2 K |
| Ambient diffraction temperature |
130 ± 2 K |
| Number of distinct elements |
5 |
| Space group number |
1 |
| Hermann-Mauguin space group symbol |
P 1 |
| Hall space group symbol |
P 1 |
| Residual factor for all reflections |
0.0857 |
| Residual factor for significantly intense reflections |
0.0519 |
| Weighted residual factors for significantly intense reflections |
0.1195 |
| Weighted residual factors for all reflections included in the refinement |
0.1282 |
| Goodness-of-fit parameter for all reflections included in the refinement |
0.911 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
Yes |
| Has Fobs |
No |
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https://www.crystallography.net/7048146.html
