Information card for entry 7048284

Structure parameters

• Formula: C29.2 H36.3 B10 Cl2 N2.1 P2 Pd
• Calculated formula: C29.2 H36.3 B10 Cl2 N2.1 P2 Pd
• Title of publication: Electronic versus steric control in palladium complexes of carboranyl phosphine-iminophosphorane ligands.
• Authors of publication: Rodríguez-Rey, José Luis; Esteban-Gómez, David; Platas-Iglesias, Carlos; Sousa-Pedrares, Antonio
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 2
• Pages of publication: 486 - 503
• a: 14.3478 ± 0.0005 Å
• b: 15.215 ± 0.0006 Å
• c: 17.8257 ± 0.0006 Å
• α: 90.742 ± 0.002°
• β: 100.401 ± 0.002°
• γ: 109.907 ± 0.002°
• Cell volume: 3587.1 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0705
• Residual factor for significantly intense reflections: 0.0423
• Weighted residual factors for significantly intense reflections: 0.0766
• Weighted residual factors for all reflections included in the refinement: 0.0867
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No