Information card for entry 7048289

Structure parameters

• Formula: C28 H35 B10 Cl2 N P2 Pd
• Calculated formula: C28 H35 B10 Cl2 N P2 Pd
• Title of publication: Electronic versus steric control in palladium complexes of carboranyl phosphine-iminophosphorane ligands.
• Authors of publication: Rodríguez-Rey, José Luis; Esteban-Gómez, David; Platas-Iglesias, Carlos; Sousa-Pedrares, Antonio
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 2
• Pages of publication: 486 - 503
• a: 12.452 ± 0.0008 Å
• b: 16.2137 ± 0.0008 Å
• c: 17.6328 ± 0.0011 Å
• α: 90°
• β: 109.186 ± 0.004°
• γ: 90°
• Cell volume: 3362.2 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0564
• Residual factor for significantly intense reflections: 0.0362
• Weighted residual factors for significantly intense reflections: 0.0708
• Weighted residual factors for all reflections included in the refinement: 0.0764
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No