Information card for entry 7048755

Structure parameters

• Formula: C63 H82 O8 P2 Pd2
• Calculated formula: C63 H82 O8 P2 Pd2
• Title of publication: The surprisingly facile formation of Pd(i)-phosphido complexes from ortho-biphenylphosphines and palladium acetate.
• Authors of publication: Montgomery, Michelle; O'Brien, Harry M; Méndez-Gálvez, Carolina; Bromfield, Caitlin R.; Roberts, Jack P. M.; Winnicka, Anna M.; Horner, Andrew; Elorriaga, David; Sparkes, Hazel A.; Bedford, Robin B.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 11
• Pages of publication: 3539 - 3542
• a: 12.7552 ± 0.0006 Å
• b: 11.4178 ± 0.0006 Å
• c: 19.7866 ± 0.0011 Å
• α: 90°
• β: 100.144 ± 0.003°
• γ: 90°
• Cell volume: 2836.6 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/n 1
• Hall space group symbol: -P 2yac
• Residual factor for all reflections: 0.0449
• Residual factor for significantly intense reflections: 0.0312
• Weighted residual factors for significantly intense reflections: 0.0646
• Weighted residual factors for all reflections included in the refinement: 0.0702
• Goodness-of-fit parameter for all reflections included in the refinement: 1.006
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No