The surprisingly facile formation of Pd(i)-phosphido complexes from ortho-biphenylphosphines and palladium acetate.
Authors of publication
Montgomery, Michelle; O'Brien, Harry M; Méndez-Gálvez, Carolina; Bromfield, Caitlin R.; Roberts, Jack P. M.; Winnicka, Anna M.; Horner, Andrew; Elorriaga, David; Sparkes, Hazel A.; Bedford, Robin B.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2019
Journal volume
48
Journal issue
11
Pages of publication
3539 - 3542
a
11.5721 ± 0.0004 Å
b
15.3228 ± 0.0005 Å
c
22.479 ± 0.0007 Å
α
85.7858 ± 0.0014°
β
75.7187 ± 0.0015°
γ
69.5539 ± 0.0015°
Cell volume
3619 ± 0.2 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0305
Residual factor for significantly intense reflections
0.0263
Weighted residual factors for significantly intense reflections
0.06
Weighted residual factors for all reflections included in the refinement
0.0618
Goodness-of-fit parameter for all reflections included in the refinement
