Information card for entry 7049286

Structure parameters

• Formula: C23 H23 Cl3 F3 Ge N O3 P S
• Calculated formula: C23 H23 Cl3 F3 Ge N O3 P S
• Title of publication: Stabilization of bis(chlorogermyliumylidene)s within bifunctional PNNP ligand frameworks and their reactivity studies.
• Authors of publication: Sahoo, Padmini; Raut, Ravindra K.; Maurya, Devesh; Kumar, Vikas; Rani, Pooja; Gonnade, Rajesh G.; Majumdar, Moumita
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 21
• Pages of publication: 7344 - 7351
• a: 10.8139 ± 0.0005 Å
• b: 17.615 ± 0.0009 Å
• c: 14.8147 ± 0.0008 Å
• α: 90°
• β: 90.808 ± 0.003°
• γ: 90°
• Cell volume: 2821.7 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1094
• Residual factor for significantly intense reflections: 0.0733
• Weighted residual factors for significantly intense reflections: 0.1698
• Weighted residual factors for all reflections included in the refinement: 0.1893
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No