Information card for entry 7049550

Structure parameters

• Formula: C32 H44 Co2 Mo10 N8 O50 Zn2
• Calculated formula: C32 H44 Co2 Mo10 N8 O50 Zn2
• Title of publication: Syntheses, structures and catalytic properties of Evans-Showell-type polyoxometalate-based 3D metal-organic complexes constructed from the semi-rigid bis(pyridylformyl)piperazine ligand and transition metals.
• Authors of publication: Li, Feng-Cai; Tan, Li-Kun; Li, Xi-Li; Kong, Hua-Jie; Ge, Li-Ming; Yue, Ling-Yu; Han, Li-Feng
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 17
• Pages of publication: 5831 - 5841
• a: 21.544 ± 0.002 Å
• b: 14.2328 ± 0.0012 Å
• c: 24.246 ± 0.003 Å
• α: 90°
• β: 104.817 ± 0.01°
• γ: 90°
• Cell volume: 7187.4 ± 1.3 ų
• Cell temperature: 298.15 K
• Ambient diffraction temperature: 298.15 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1109
• Residual factor for significantly intense reflections: 0.0921
• Weighted residual factors for significantly intense reflections: 0.2025
• Weighted residual factors for all reflections included in the refinement: 0.2129
• Goodness-of-fit parameter for all reflections included in the refinement: 1.091
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No