Information card for entry 7050466

Structure parameters

• Formula: C52 H44 Co2 N8 O18 P2 V4
• Calculated formula: C52 H40 Co2 N8 O18 P2 V4
• Title of publication: Hydrothermal synthesis and crystal structure of two hetero-transition metal polymers: [Co(1,10-phen)2(V2O4) (O3PCH2CH2CH2PO3)]n and [{Co(1,10-phen)2}2(V4O10) (O3PCH2CH2CH2CH2PO3)(2H2O)]n
• Authors of publication: Fu, Rui-Biao; Hu, Sheng-Min; Fu, Zhi-Yong; Zhang, Jian-Jun; Wu, Xin-Tao
• Journal of publication: New Journal of Chemistry
• Year of publication: 2003
• Journal volume: 27
• Journal issue: 2
• Pages of publication: 230
• a: 10.2132 ± 0.0003 Å
• b: 11.7055 ± 0.0005 Å
• c: 12.3666 ± 0.0005 Å
• α: 75.594 ± 0.002°
• β: 82.445 ± 0.002°
• γ: 86.071 ± 0.002°
• Cell volume: 1418.53 ± 0.09 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0872
• Residual factor for significantly intense reflections: 0.0567
• Weighted residual factors for significantly intense reflections: 0.1029
• Weighted residual factors for all reflections included in the refinement: 0.1197
• Goodness-of-fit parameter for all reflections included in the refinement: 1.106
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No