Information card for entry 7051206

Structure parameters

• Formula: C5 H14 N8 Ni
• Calculated formula: C5 H14 N8 Ni
• Title of publication: Synthesis of N3−/SCN− bridged polynuclear complexes of nickel(II) using N,N,N'-trimethylethane-1,2-diamine as a blocking ligand: low temperature magnetic study and single crystal structure of [Ni(μ1,1-N3)(μ1,3-N3)(N,N,N'-Me3en)]n
• Authors of publication: Montserrat Monfort; Inmaculada Resino; Joan Ribas; Xavier Solans; Mercé Font-Bardia
• Journal of publication: New J. Chem.
• Year of publication: 2001
• Journal volume: 25
• Journal issue: 12
• Pages of publication: 1577 - 1582
• a: 7.132 ± 0.004 Å
• b: 10.122 ± 0.002 Å
• c: 14.614 ± 0.005 Å
• α: 90°
• β: 102.22 ± 0.02°
• γ: 90°
• Cell volume: 1031.1 ± 0.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1373
• Residual factor for significantly intense reflections: 0.0504
• Weighted residual factors for all reflections: 0.1395
• Weighted residual factors for significantly intense reflections: 0.1008
• Goodness-of-fit parameter for all reflections: 1.005
• Goodness-of-fit parameter for significantly intense reflections: 1.07
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No