Information card for entry 7052684

Structure parameters

• Formula: C58 H42 B F24 N7 Rh
• Calculated formula: C58 H42 B F24 N7 Rh
• Title of publication: Rhodium(i) complexes bearing N-donor ligands: catalytic activity towards intramolecular cyclization of alkynoic acids and ligand lability
• Authors of publication: Man, Bradley Y.-W.; Bhadbhade, Mohan; Messerle, Barbara A.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2011
• Journal volume: 35
• Journal issue: 8
• Pages of publication: 1730
• a: 40.121 ± 0.002 Å
• b: 12.7579 ± 0.0007 Å
• c: 24.5524 ± 0.0012 Å
• α: 90°
• β: 102.969 ± 0.001°
• γ: 90°
• Cell volume: 12246.8 ± 1.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0726
• Residual factor for significantly intense reflections: 0.0575
• Weighted residual factors for significantly intense reflections: 0.1734
• Weighted residual factors for all reflections included in the refinement: 0.186
• Goodness-of-fit parameter for all reflections included in the refinement: 1.373
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No