Information card for entry 7053445

Structure parameters

• Formula: C30.4 H28.8 B Cl0.8 F4 N P Rh
• Calculated formula: C30.4 H28.8 B Cl0.8 F4 N P Rh
• Title of publication: 2-(2′-Pyridyl)-4,6-diphenylphosphinine versus 2-(2′-pyridyl)-4,6-diphenylpyridine: an evaluation of their coordination chemistry towards Rh(i)
• Authors of publication: Carrasco, Ariadna Campos; Pidko, Evgeny A.; Masdeu-Bultó, Anna M.; Lutz, Martin; Spek, Anthony L.; Vogt, Dieter; Müller, Christian
• Journal of publication: New Journal of Chemistry
• Year of publication: 2010
• Journal volume: 34
• Journal issue: 8
• Pages of publication: 1547
• a: 9.7987 ± 0.0002 Å
• b: 10.3575 ± 0.0002 Å
• c: 14.5382 ± 0.0003 Å
• α: 84.875 ± 0.0006°
• β: 85.4051 ± 0.0006°
• γ: 71.0572 ± 0.0008°
• Cell volume: 1387.95 ± 0.05 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0586
• Residual factor for significantly intense reflections: 0.0396
• Weighted residual factors for significantly intense reflections: 0.0872
• Weighted residual factors for all reflections included in the refinement: 0.0949
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No