Information card for entry 7053733

Structure parameters

• Formula: C49.59 H52.85 N11 O13.84 Pr
• Calculated formula: C49.586 H50.3452 N11 O13.828 Pr
• Title of publication: A lanthanide-based helicate coordination polymer derived from a rigid monodentate organic bridge synthesized in the solid state
• Authors of publication: Bučar, Dejan-Krešimir; Papaefstathiou, Giannis S.; Hamilton, Tamara D.; MacGillivray, Leonard R.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2008
• Journal volume: 32
• Journal issue: 5
• Pages of publication: 797
• a: 23.02 ± 0.003 Å
• b: 16.8687 ± 0.0018 Å
• c: 13.8344 ± 0.0015 Å
• α: 90°
• β: 96.593 ± 0.005°
• γ: 90°
• Cell volume: 5336.6 ± 1.1 ų
• Cell temperature: 200 ± 1 K
• Ambient diffraction temperature: 200 ± 1 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0425
• Residual factor for significantly intense reflections: 0.0332
• Weighted residual factors for significantly intense reflections: 0.0696
• Weighted residual factors for all reflections included in the refinement: 0.072
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No