Information card for entry 7053887

Structure parameters

• Formula: C48 H53 Cu Mo12 N20 O44 P
• Calculated formula: C48 H44 Cu Mo12 N20 O44 P
• Title of publication: Two novel zipper-like compounds of the usual and bivanadyl capped Keggin clusters connected by propeller-shaped complexes
• Authors of publication: Yu, Yan; Ma, Huiyuan; Pang, Haijun; Li, Shaobin; Yu, Tingting; Liu, Heng; Zhao, Chunyan; Zhang, Zhuanfang
• Journal of publication: New Journal of Chemistry
• Year of publication: 2014
• Journal volume: 38
• Journal issue: 3
• Pages of publication: 1271
• a: 22.04 ± 0.005 Å
• b: 14.85 ± 0.005 Å
• c: 24.821 ± 0.005 Å
• α: 90°
• β: 100.605 ± 0.005°
• γ: 90°
• Cell volume: 7985 ± 4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1074
• Residual factor for significantly intense reflections: 0.0877
• Weighted residual factors for significantly intense reflections: 0.21
• Weighted residual factors for all reflections included in the refinement: 0.2189
• Goodness-of-fit parameter for all reflections included in the refinement: 0.973
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No