Information card for entry 7054353

Structure parameters

• Formula: C18 H17 N5 O7 Pb
• Calculated formula: C18 H15 N5 O7 Pb
• Title of publication: Dynamic crystal-to-crystal transformation of 1D to 2D lead(ii) coordination polymers by de- and rehydration with no change in the morphology of nano-particles
• Authors of publication: Hashemi, Lida; Morsali, Ali; Marandi, Farzin; Pantenburg, Ingo; Azhdari Tehrani, Alireza
• Journal of publication: New Journal of Chemistry
• Year of publication: 2014
• Journal volume: 38
• Journal issue: 8
• Pages of publication: 3375
• a: 9.3542 ± 0.0014 Å
• b: 11.1933 ± 0.0016 Å
• c: 11.963 ± 0.0018 Å
• α: 62.314 ± 0.011°
• β: 68.905 ± 0.012°
• γ: 73.544 ± 0.011°
• Cell volume: 1024.6 ± 0.3 ų
• Cell temperature: 170 ± 2 K
• Ambient diffraction temperature: 170 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0569
• Residual factor for significantly intense reflections: 0.0484
• Weighted residual factors for significantly intense reflections: 0.1311
• Weighted residual factors for all reflections included in the refinement: 0.1403
• Goodness-of-fit parameter for all reflections included in the refinement: 1.088
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7054263
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No