Information card for entry 7054948

Structure parameters

• Formula: C88 H148 N6 O9 Si4 Yb2
• Calculated formula: C88 H148 N6 O9 Si4 Yb2
• Title of publication: Synthesis and characterization of bis(amidate) rare-earth metal amides and their application in catalytic addition of amines to carbodiimides
• Authors of publication: Cheng, Hao; Xiao, Yang; Lu, Chengrong; Zhao, Bei; Wang, Yaorong; Yao, Yingming
• Journal of publication: New J. Chem.
• Year of publication: 2015
• Journal volume: 39
• Journal issue: 10
• Pages of publication: 7667
• a: 13.7 ± 0.016 Å
• b: 14 ± 0.03 Å
• c: 15.31 ± 0.02 Å
• α: 109.37 ± 0.04°
• β: 105.895 ± 0.008°
• γ: 98.64 ± 0.02°
• Cell volume: 2569 ± 7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0601
• Residual factor for significantly intense reflections: 0.0492
• Weighted residual factors for significantly intense reflections: 0.1178
• Weighted residual factors for all reflections included in the refinement: 0.1272
• Goodness-of-fit parameter for all reflections included in the refinement: 1.085
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No