Supramolecular frameworks of binuclear dioxomolybdenum(vi) complexes with ONS donor ligands using 4,4′-azopyridine as a pillar: crystal structure, DFT calculations and biological study
Authors of publication
Biswal, Debanjana; Pramanik, Nikhil Ranjan; Chakrabarti, Syamal; Drew, Michael G. B.; Mitra, Payel; Acharya, Krishnendu; Biswas, Sujan; Mondal, Tapan Kumar
Journal of publication
New J. Chem.
Year of publication
2015
Journal volume
39
Journal issue
11
Pages of publication
8681
a
10.9255 ± 0.0007 Å
b
10.9637 ± 0.0007 Å
c
13.2353 ± 0.0008 Å
α
67.269 ± 0.006°
β
69.255 ± 0.005°
γ
67.937 ± 0.006°
Cell volume
1314 ± 0.16 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
7
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0822
Residual factor for significantly intense reflections
0.059
Weighted residual factors for significantly intense reflections
0.1243
Weighted residual factors for all reflections included in the refinement
0.1387
Goodness-of-fit parameter for all reflections included in the refinement
