V(iv), Fe(ii), Ni(ii) and Cu(ii) complexes bearing 2,2,2-tris(pyrazol-1-yl)ethyl methanesulfonate: application as catalysts for the cyclooctane oxidation
Authors of publication
Silva, Telma F. S.; Rocha, Bruno G. M.; Guedes da Silva, M. Fátima C.; Martins, Luísa M. D. R. S.; Pombeiro, Armando J. L.
Journal of publication
New J. Chem.
Year of publication
2016
Journal volume
40
Journal issue
1
Pages of publication
528
a
8.2321 ± 0.0007 Å
b
9.8695 ± 0.0008 Å
c
12.5776 ± 0.001 Å
α
101.763 ± 0.003°
β
103.543 ± 0.002°
γ
100.003 ± 0.003°
Cell volume
945.92 ± 0.14 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
7
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1003
Residual factor for significantly intense reflections
0.0679
Weighted residual factors for significantly intense reflections
0.1943
Weighted residual factors for all reflections included in the refinement
0.2237
Goodness-of-fit parameter for all reflections included in the refinement
