Design, structures and study of non-covalent interactions of mono-, di-, and tetranuclear complexes of a bifurcated quadridentate tripod ligand, N-(aminopropyl)-diethanolamine
Authors of publication
Sama, Farasha; Ansari, Istikhar A.; Raizada, Mukul; Ahmad, Musheer; Nagaraja, C. M.; Shahid, M.; Kumar, Abhinav; Khan, Kulsum; Siddiqi, Zafar A.
Journal of publication
New J. Chem.
Year of publication
2017
Journal volume
41
Journal issue
5
Pages of publication
1959
a
8.6719 ± 0.0007 Å
b
10.0649 ± 0.0007 Å
c
11.3026 ± 0.0007 Å
α
89.096 ± 0.005°
β
79.802 ± 0.006°
γ
65.87 ± 0.007°
Cell volume
884.33 ± 0.12 Å3
Cell temperature
296 ± 2 K
Ambient diffraction temperature
296 ± 2 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0534
Residual factor for significantly intense reflections
0.041
Weighted residual factors for significantly intense reflections
0.0964
Weighted residual factors for all reflections included in the refinement
0.1062
Goodness-of-fit parameter for all reflections included in the refinement
