Information card for entry 7056154

Structure parameters

• Formula: C50 H46 O14 Si10
• Calculated formula: C50 H46 O14 Si10
• Title of publication: Unusual cis and trans architecture of dihydrofunctional double-decker shaped silsesquioxane and synthesis of its ethyl bridged π-conjugated arene derivatives
• Authors of publication: Walczak, M.; Januszewski, R.; Majchrzak, M.; Kubicki, M.; Dudziec, B.; Marciniec, B.
• Journal of publication: New J. Chem.
• Year of publication: 2017
• Journal volume: 41
• Journal issue: 9
• Pages of publication: 3290
• a: 10.5118 ± 0.0005 Å
• b: 13.8528 ± 0.0008 Å
• c: 19.5175 ± 0.0006 Å
• α: 98.402 ± 0.004°
• β: 90.407 ± 0.003°
• γ: 90.95 ± 0.004°
• Cell volume: 2811.1 ± 0.2 ų
• Cell temperature: 130 ± 1 K
• Ambient diffraction temperature: 130 ± 1 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0725
• Residual factor for significantly intense reflections: 0.0472
• Weighted residual factors for significantly intense reflections: 0.125
• Weighted residual factors for all reflections included in the refinement: 0.1361
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No