Information card for entry 7056276

Structure parameters

• Chemical name: [RuCl(propionylhydrazine)(?6-p-cymene)]Cl
• Formula: C13 H22 Cl2 N2 O Ru
• Calculated formula: C13 H22 Cl2 N2 O Ru
• Title of publication: Conversion of hydrazides into N,N'-diacylhydrazines in the presence of ruthenium(II)-arene complex
• Authors of publication: Nikolić, Stefan; Ćirić, Ivanka; Roller, Alexander; Lukes, Vladimir; Arion, Vladimir; Grguric-Sipka, Sanja
• Journal of publication: New J. Chem.
• Year of publication: 2017
• Journal volume: 41
• Journal issue: 14
• Pages of publication: 6857 - 6865
• a: 13.8233 ± 0.0006 Å
• b: 20.4127 ± 0.0009 Å
• c: 12.0459 ± 0.0005 Å
• α: 90°
• β: 103.277 ± 0.0016°
• γ: 90°
• Cell volume: 3308.2 ± 0.2 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0353
• Residual factor for significantly intense reflections: 0.0298
• Weighted residual factors for significantly intense reflections: 0.0752
• Weighted residual factors for all reflections included in the refinement: 0.0782
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No