The molecular design of cage metal complexes for biological applications: pathways of the synthesis, and X-ray structures of a series of new N2-, S2- and O2-alicyclic iron(ii) di- and tetrachloroclathrochelates
Authors of publication
Zelinskii, Genrikh E.; Belov, Alexander S.; Belaya, Irina G.; Vologzhanina, Anna V.; Novikov, Valentin V.; Varzatskii, Oleg A.; Voloshin, Yan Z.
Journal of publication
New Journal of Chemistry
Year of publication
2018
Journal volume
42
Journal issue
1
Pages of publication
56
a
14.486 ± 0.0004 Å
b
15.3721 ± 0.0003 Å
c
15.7873 ± 0.0004 Å
α
117.417 ± 0.001°
β
99.084 ± 0.002°
γ
107.035 ± 0.001°
Cell volume
2800.59 ± 0.13 Å3
Cell temperature
120 K
Ambient diffraction temperature
120 K
Number of distinct elements
8
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0644
Residual factor for significantly intense reflections
0.0506
Weighted residual factors for significantly intense reflections
0.0981
Weighted residual factors for all reflections included in the refinement
0.1043
Goodness-of-fit parameter for all reflections included in the refinement
