Crystallography Open Database

Information card for entry 7056936

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Coordinates	7056936.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H32.04 B9 Cl2.04 P
Calculated formula	C24 H32.0441 B9 Cl2.0441 P
Title of publication	Diverse chemistry of the dianion [closo-B9H9]2−: synthesis and reactivity of its mono-anionic derivative [arachno-B9H12-4,8-Cl2]−
Authors of publication	Schlüter, Florian; Bernhardt, Eduard; Zhizhin, Konstantin
Journal of publication	New Journal of Chemistry
Year of publication	2018
Journal volume	42
Journal issue	4
Pages of publication	2553
a	23.2777 ± 0.0007 Å
b	10.3096 ± 0.0002 Å
c	25.1059 ± 0.0008 Å
α	90°
β	110.776 ± 0.004°
γ	90°
Cell volume	5633.2 ± 0.3 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0435
Residual factor for significantly intense reflections	0.0368
Weighted residual factors for significantly intense reflections	0.0942
Weighted residual factors for all reflections included in the refinement	0.0986
Goodness-of-fit parameter for all reflections included in the refinement	1.071
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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