Design and synthesis of imidazoles linearly connected to carbocyclic and heterocyclic ringsviaa 1,2,3-triazole linker. Reactivity of β-azolyl enamines towards heteroaromatic azides
Authors of publication
Beliaev, Nikolai A.; Shafikov, Marsel Z.; Efimov, Ilya V.; Beryozkina, Tetyana V.; Lubec, Gert; Dehaen, Wim; Bakulev, Vasiliy A.
Journal of publication
New Journal of Chemistry
Year of publication
2018
Journal volume
42
Journal issue
9
Pages of publication
7049
a
7.0876 ± 0.0008 Å
b
9.8869 ± 0.0013 Å
c
11.4194 ± 0.0015 Å
α
89.761 ± 0.016°
β
73.244 ± 0.011°
γ
69.093 ± 0.012°
Cell volume
711.41 ± 0.18 Å3
Cell temperature
295 ± 2 K
Ambient diffraction temperature
295 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1315
Residual factor for significantly intense reflections
0.0439
Weighted residual factors for significantly intense reflections
0.0691
Weighted residual factors for all reflections included in the refinement
0.0752
Goodness-of-fit parameter for all reflections included in the refinement
