Information card for entry 7057474

Structure parameters

• Common name: [Rh(n5-C5Me5)(pin)Cl](Cl)
• Formula: C33 H50 Cl4 N4 O Rh2
• Calculated formula: C33 H50 Cl4 N4 O Rh2
• Title of publication: Structural and solution equilibrium studies on half-sandwich organorhodium complexes of (N,N) donor bidentate ligands
• Authors of publication: Mészáros, János P.; Dömötör, Orsolya; Hackl, Carmen M.; Roller, Alexander; Keppler, Bernhard K.; Kandioller, Wolfgang; Enyedy, Éva A.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2018
• Journal volume: 42
• Journal issue: 13
• Pages of publication: 11174
• a: 8.6742 ± 0.0003 Å
• b: 14.5573 ± 0.0006 Å
• c: 14.6705 ± 0.0006 Å
• α: 90°
• β: 104.111 ± 0.0013°
• γ: 90°
• Cell volume: 1796.59 ± 0.12 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0224
• Residual factor for significantly intense reflections: 0.0192
• Weighted residual factors for significantly intense reflections: 0.0474
• Weighted residual factors for all reflections included in the refinement: 0.0494
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No