Information card for entry 7058101

Structure parameters

• Formula: Cr3 Cs6 Ge3 K4.5 Na7 O136.5 Tb3 W30
• Calculated formula: Cr3 Cs6 Ge3 K4.5 Na7 O136.5 Tb3 W30
• Title of publication: Two rare Cr‒Ln (Ln = Dy, Tb) heterometallic cluster substituted polyoxometalates featuring hexameric aggregates: hydrothermal syntheses, crystal structures and magnetic studies
• Authors of publication: Gu, Ya-Nan; Yu, Hao; Lin, Li-Dan; Wu, Yan-Lan; Li, Zhong; Pan, Wen-Yue; He, Jiang; Chen, Ling; Li, Qi; Li, Xin-Xiong
• Journal of publication: New Journal of Chemistry
• Year of publication: 2019
• Journal volume: 43
• Journal issue: 7
• Pages of publication: 3011
• a: 29.0355 ± 0.0011 Å
• b: 29.0355 ± 0.0011 Å
• c: 32.8451 ± 0.0013 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 23980.6 ± 1.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0393
• Residual factor for significantly intense reflections: 0.031
• Weighted residual factors for significantly intense reflections: 0.0744
• Weighted residual factors for all reflections included in the refinement: 0.0773
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No