Information card for entry 7058108

Structure parameters

• Formula: C50.52 H66 Br4 Cl1.48 N8.52 Ni2 O14 Pb2 S2.52
• Calculated formula: C50.514 H58 Br4 Cl1.486 N8.514 Ni2 O14 Pb2 S2.514
• Title of publication: A tetranuclear nickel/lead complex with a salen type Schiff base: synthesis, structure and exploration of photosensitive Schottky barrier diode behaviour
• Authors of publication: Roy, Sourav; Dey, Arka; Drew, Michael G. B.; Ray, Partha Pratim; Chattopadhyay, Shouvik
• Journal of publication: New Journal of Chemistry
• Year of publication: 2019
• Journal volume: 43
• Journal issue: 13
• Pages of publication: 5020
• a: 38.41 ± 0.003 Å
• b: 38.41 ± 0.003 Å
• c: 12.7948 ± 0.0011 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 16348 ± 2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 9
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.1271
• Residual factor for significantly intense reflections: 0.0722
• Weighted residual factors for significantly intense reflections: 0.1178
• Weighted residual factors for all reflections included in the refinement: 0.1346
• Goodness-of-fit parameter for all reflections included in the refinement: 0.989
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No